羡瑜, 王翠翠, 王戈, 程海涛. 芯壳结构竹塑复合材料断口冲击强度的分形表征[J]. 农业工程学报, 2015, 31(12): 295-300. DOI: 10.11975/j.issn.1002-6819.2015.12.040
    引用本文: 羡瑜, 王翠翠, 王戈, 程海涛. 芯壳结构竹塑复合材料断口冲击强度的分形表征[J]. 农业工程学报, 2015, 31(12): 295-300. DOI: 10.11975/j.issn.1002-6819.2015.12.040
    Xian Yu, Wang Cuicui, Wang Ge, Cheng Haitao. Fractal characterization of impact strength fracture of bamboo plastic composites with core-shell structure[J]. Transactions of the Chinese Society of Agricultural Engineering (Transactions of the CSAE), 2015, 31(12): 295-300. DOI: 10.11975/j.issn.1002-6819.2015.12.040
    Citation: Xian Yu, Wang Cuicui, Wang Ge, Cheng Haitao. Fractal characterization of impact strength fracture of bamboo plastic composites with core-shell structure[J]. Transactions of the Chinese Society of Agricultural Engineering (Transactions of the CSAE), 2015, 31(12): 295-300. DOI: 10.11975/j.issn.1002-6819.2015.12.040

    芯壳结构竹塑复合材料断口冲击强度的分形表征

    Fractal characterization of impact strength fracture of bamboo plastic composites with core-shell structure

    • 摘要: 为了定量表征不同壳层材料对芯壳结构竹塑复合材料冲击断口复杂程度的影响,以造纸剩余物竹屑和高密度聚乙烯(high density polyethylene,HDPE)作为芯层材料,以纯HDPE、竹浆纤维/HDPE、纳米碳酸钙/HDPE和白泥/HDPE分别作为壳层材料,采用熔融共挤工艺制备芯壳结构竹塑复合材料。在室温(23℃)环境下,测试了复合材料无缺口冲击强度,采用扫描电镜对4种不同壳层材料断口进行形貌分析,基于分形理论和图像处理技术,运用像素点法计算了复合材料的冲击断口表面分形维数,考察了复合材料断口表面分形维数和冲击强度的关系。结果表明,不同壳层材料的芯壳结构竹塑复合材料冲击断口表面分形维数存在一定差异,壳层为HDPE的复合材料断口表面分形维数最大,为2.2204,壳层为白泥/ HDPE的分形维数最小,为2.2075。不同壳层复合材料冲击断口表面分形维数拟合曲线的决定系数均大于0.98,说明复合材料断口表面分形特征显著。并且,复合材料断口表面分形维数与冲击强度之间拟合曲线的决定系数为0.9857,近似呈指数函数关系。研究结果为进一步深入研究芯壳结构竹塑复合材料的表面微观结构提供参考。

       

      Abstract: Abstract: In order to study the rupture mechanism of the bamboo plastic composites (BPCs) with core-shell structure, in this paper bamboo residue fibers and high density polyethylene (HDPE) were used as materials of core layer; HDPE, bamboo pulp fibers/HDPE, nano-CaCO3/HDPE and white mud/HDPE, were respectively used as materials of shell layer to manufacture the BPCs with core-shell structure by coextrusion technology. The ratios of bamboo pulp fibers, nano-CaCO3 and white mud to HDPE in the shell layer structure were to be 10:90 respectively. To present the theoretical relationship between fractal dimensions (D) and the impact strength (?), and analyze the effects of different shell layer materials on the impact strength in the BPCs with core-shell structure, Charpy non-notched impact strength of the BPCs with core-shell structure was measured at room temperature according to ASTMD6110-2010. The fractographs of the BPCs with core-shell structure that had different shell layer materials were observed by scanning electron microscope (SEM). The impact fracture surface topography of BPCs manifested self-similarity. Based on fractal theory and computer image processing technology, a MATLAB program which computed the fracture's box-counting dimension of the BPCs with core-shell structure was designed. The digital image was transformed into factual image, and the charpy impact fracture surface fractal dimensions of the BPCs with core-shell structure that had different shell layer materials were measured by pixel-covering method, to investigate the relationship between impact strength and fractal dimension of the BPCs with core-shell structure. Results showed that the BPCs fracture possessed fractal characteristics and there were differences for the fractal dimensions of the BPCs with core-shell structure that had different shell layer materials. The fractal dimensions of the fracture surface were within the range of from 2.2075 to 2.2204, the linear degree of fitted beeline of MATLAB program was high and the correlation coefficients obtained were more than 0.98. The strong linear correlation indicated that impact fracture surface of the BPCs with core-shell structure had significant fractal characteristics. The impact fracture topography of HDPE in the shell layer was the most complicated in 4 kinds of fractures of the BPCs with core-shell structure, and the fractal dimension was up to 2.2204; the impact fracture topography of white mud/HDPE in the shell layer was more regular, and the fractal dimension was the smallest. The results accorded with the observed results by human eyes. The impact strength of the BPCs with core-shell structure containing HDPE shell layer material was the best and that containing white mud/HDPE had the worst performances. And the relationship between impact strength and fracture surface fractal dimension of the BPCs with core-shell structure obeyed exponential function roughly. Thus using the fractal dimensions to describe the impact fracture surface morphology of the BPCs with core-shell structure may provide a new approach to investigate the inherence rule between fractal characteristics and charpy impact strength of the BPCs with core-shell structure.

       

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