陈计远, 王粮局, 王红英, 张国栋. 鱼膨化饲料热风干燥动力学模型及湿热特性[J]. 农业工程学报, 2021, 37(14): 317-322. DOI: 10.11975/j.issn.1002-6819.2021.14.037
    引用本文: 陈计远, 王粮局, 王红英, 张国栋. 鱼膨化饲料热风干燥动力学模型及湿热特性[J]. 农业工程学报, 2021, 37(14): 317-322. DOI: 10.11975/j.issn.1002-6819.2021.14.037
    Chen Jiyuan, Wang Liangju, Wang Hongying, Zhang Guodong. Drying kinetic model and hygrothermal characteristics of fish extruded feed during hot air drying[J]. Transactions of the Chinese Society of Agricultural Engineering (Transactions of the CSAE), 2021, 37(14): 317-322. DOI: 10.11975/j.issn.1002-6819.2021.14.037
    Citation: Chen Jiyuan, Wang Liangju, Wang Hongying, Zhang Guodong. Drying kinetic model and hygrothermal characteristics of fish extruded feed during hot air drying[J]. Transactions of the Chinese Society of Agricultural Engineering (Transactions of the CSAE), 2021, 37(14): 317-322. DOI: 10.11975/j.issn.1002-6819.2021.14.037

    鱼膨化饲料热风干燥动力学模型及湿热特性

    Drying kinetic model and hygrothermal characteristics of fish extruded feed during hot air drying

    • 摘要: 热风干燥是水产膨化饲料加工过程中极为重要的工序。为了探究水产膨化饲料在热风干燥过程中的湿热特性变化规律,该研究以草鱼(成鱼)膨化饲料为对象,设置热风温度(60~100 ℃)和风速(0.5~1.5 m/s)2个试验因素,在自行设计的热风干燥机上进行干燥试验。结果表明,在同一风速条件下,饲料的干燥速率随着热风温度的升高而显著增大(P<0.01)。同样的,在同一热风温度条件下,增大风速可以提高干燥速率。使用Verma模型拟合上述试验数据,决定系数(R2)、离差平方和(χ2)、均方根误差(RMSE)和平均相对误差(e)的计算结果表明该模型对草鱼膨化饲料在不同干燥条件下的试验数据具有较高的预测精度。同时分别建立了Verma模型参数关于热风温度和风速的回归模型,且回归模型R2均大于0.979。低场核磁共振(Low-Field Nuclear Magnetic Resonance analysis,LF-NMR)的横向弛豫时间(T2)谱显示,随着干燥过程的进行,T21峰面积逐渐减小,即不易流动水占比显著减少(P<0.01);而且弛豫曲线有整体向左偏移的趋势,说明水分与底物的结合更加紧密,自由度降低。红外热像图显示,在干燥时间为5 min时,饲料出现了边角效应;在干燥时间为15 min和20 min时,部分中心处饲料出现了过热效应。上述研究可为草鱼膨化饲料干燥工艺参数的选择提供参考,并为其他种类水产饲料热风干燥湿热特性的研究提供新思路。

       

      Abstract: Abstract: Processing parameters during drying are highly critical to the quality and yield of extruded aquatic feed. Taking grass carp (adult fish) extruded feed as the research object, this study aims to explore the hygrothermal characteristics of fish feed in the process of hot air drying. An experimental box was also selected to simulate the temperature and moisture content in the extruder. The measured temperature of fish feed was 90.11±1.31 ℃, and the measured moisture content of dry basis was 24.02%±0.98%. Two experimental parameters were set, including the air temperature (60-100 ℃) and air velocity (0.5-1.5 m/s). The drying experiment was performed on a self-developed hot air dryer, where a load cell with the accuracy of 0.01g was selected to accurately record the moisture of fish feed during drying. An infrared thermal imager was used to observe the temperature distribution of fish feed. Low-field nuclear magnetic resonance analysis (LF-NMR) was also utilized to explore the change of water state in the fish feed. The samples were taken every 20 minutes for the LF-NMR during the test, where the main magnetic field strength was 0.5T, and the resonance frequency was 21 MHz. Among them, a Carr-Purcell-Meiboom-Gill (CPMG) pulse sequence was adopted to quantify the LF-NMR parameters. The results showed that there was a reduced rate drying stage in the drying process of feed in this experiment, rather than the typical constant rate drying stage. The drying rate of feed increased significantly, with the increase of air temperature (P<0.01) under the same air velocity. Similarly, the air velocity improved the drying rate at the same temperature as hot air. A Verma model was used to fit the obtained experimental data. The calculated values of R2, χ2, RMSE, and e showed that the model presented a high prediction accuracy for the experimental data of grass carp feed under different drying conditions. The Verma model parameters, k0, k1, and a, were achieved on the air temperature and air velocity, where R2 of the regression model was greater than 0.979. Transverse relaxation time (T2) spectra showed that the proportion of immobilized water in the feed was the largest in the initial stage of the drying process. Specifically, the peak area of T21 decreased gradually with the drying proceeded, indicating the proportion of immobilized water decreased significantly (P<0.01). Moreover, the whole transverse relaxation time tended to shift to the left, indicating that the combination of water and substrate was closer, and the free degree was lower. The total area of T20, T21, and T22 peaks was the smallest, while, the moisture content was the lowest at the end of drying. The infrared thermographs showed that the corner effect appeared at 5 min, particularly that some feed in the center presented the overheating at 15 and 20 min. The finding can provide a promising reference to optimize the processing parameters of grass carp extruded feed during hot air drying, together with a new idea for the study on the hygrothermal characteristics of aquatic feed.

       

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