奶牛粪固形物热风干燥特性及工艺参数优化

    Hot-air drying characteristics and optimization of the process parameters for the solid fraction of dairy manure

    • 摘要: 为了研究奶牛粪固形物在不同干燥条件下的热风干燥特性,该研究选取干燥温度、粪层厚度和搅拌频率作为研究因素,研究了牛粪干基含水率和干燥速率随时间变化的规律,利用6种经典的薄层干燥模型对牛粪的水分比与时间t曲线进行拟合获取了最优干燥模型,计算得出有效扩散系数和干燥活化能,并通过正交试验获取了干燥效率最高的快速干燥工艺参数。结果表明:干燥温度越高,粪层厚度越小,搅拌频率间隔时间越短,干基含水率下降越快;干燥过程由加速干燥阶段、近似恒速干燥阶段和降速干燥阶段组成,加速干燥阶段时间较短,符合高湿多孔类型物料的干燥特性;模型Wang and Singh能够较好地反映牛粪干燥过程水分变化规律,且有效扩散系数最小为7.31×10-5 m2/h,最小活化能为14.596 kJ/mol;通过正交试验得出干燥温度为105 ℃、粪层厚度为6 cm、搅拌频率间隔为4 min时,干燥效率最高,为0.017 h/g。该研究结果可为后续牛粪快速干燥工艺优化及干燥设备设计提供理论依据和数据支撑。

       

      Abstract: A large amount of dairy manure has posed a great threat to the environmental pollution (air, water, and soil) in the large-scale intensive dairy farming in China. Taking the dairy manure as a bedding material, some new types of manure treatment have been implemented to improve the internal resources recycling in the dairy husbandry industry at present. The safe moisture content of dairy manure is required normally 40%-50% or less for the dairy bedding material. But the high moisture content (about 75%) has been confined to the extending of dairy manure after the solid-liquid separation. Furthermore, the dairy manure is characterized by a kind of high-humidity porous material with a high free water content and dry heat conductivity. Therefore, a drying process of dairy manure can be a necessary step to fully meet the safety standards of dairy bedding materials. This study aims to optimize the process parameters and hot-air drying characteristics of the dairy manure solids under different drying conditions. Some factors were selected, including the drying temperature (60, 75, 90 and 105 ℃), the thickness of the manure layer (15, 30, 45 and 60 mm), and the duration of mixing frequency (2, 4, 6 and 8 min). The moisture content and drying rate were also measured for the dry matter in the dairy manure. The drying and weighing procedures were carried out as follows. In drying, after deforesting with at the room temperature for 12 hours, the dairy manure was put into a square stainless-steel tray with a specified thickness, where the hot-air drying test was carried out under different conditions. In weighing, the dairy manure was taken out of the drying oven every 30 minutes, and then weighed with an electronic balance, where the mass of the dairy manure was recorded. The drying test was stopped until the moisture content of the dry matter basis in the dairy manure was under 1 g/g (the moisture content of the wet matter basis was 50%). After that, six representative thin-layer drying models were applied to simulate the effective diffusion coefficient and activation energy of the drying process. An orthogonal test was also designed for the process parameters of rapid drying with the highest drying efficiency. The results showed that the higher the drying temperature was, the smaller the dairy manure thickness was, and the shorter the mixing frequency interval was, the faster the dry matter basis moisture content decreased. Moreover, the drying process of dairy manure was divided into three periods: an accelerated drying, an approximate constant-rate drying, and a falling rate period, indicating a better consistence with the drying characteristics of high-humidity porous materials. The Wang and Singh model was more suitable for the drying process of dairy manure, where the minimum effective diffusion coefficient was 7.31×10-5 m2/h, the minimum activation energy was 14.596 kJ/mol, and the orthogonal test results showed that 0.017 h/g, when the drying temperature was 105 ℃, the manure thickness was 6 cm, and the mixing frequency interval was 4 min. The finding can provide a theoretical data support to optimize the rapid drying process of dairy manure.

       

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