花椒籽油精炼工艺的试验研究

    Experimental study of zanthoxylum seed oil refining process

    • 摘要: 为将游离脂肪酸和蜡含量高的花椒籽毛油精炼为符合国家相关标准的食用油,该文通过溶剂萃取与常规碱炼结合脱酸,再用活性炭脱色。花椒籽油精炼试验结果表明:精炼油的得率73.84%,油品的酸值(以kOH计)<0.5?mg/g))达到了国家一级食用油的标准,保留了全部的α-亚麻酸,得到花椒籽毛油质量19.19%的游离脂肪酸和蜡,炼耗酸值比0.74,乙醇回收率91.15%。花椒籽油精炼优化工艺是:采用95%的乙醇与花椒籽毛油按2.5:1(V/W)的比例萃取2次花椒籽毛油,然后对萃取后的花椒籽油碱炼脱酸一次,再用活性炭脱色。

       

      Abstract: The objective of the study is to make crude zanthoxylum seed oil that contains much free fatty acid and wax. In the study the acid contained in the oil was eliminated through solvent extraction and common alkali?refining, then the oil was decolorized with activated carbon. Experiment result showed that the oil output was 73.84%, the acid value of the oil (kOH as reference) was lower than 0.5 mg/g, which reached the national standard for the first grade cooking oil, the α-LNA contained was totally reserved, the weight of ecycled free fatty acid and wax was 19.19% of zanthoxylum seed, the?ratio?of oil acid values was 0.74, and the recycling rate of ethanol was 91.15%. The improved refining process of zanthoxylum seed oil is to extract crude oil with 95% ethanol twice according to the proportion of 2.5:1(V/W) firstly, and then deacidify the oil through alkali?refining, finally?decolorize the oil with activated carbon.

       

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